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U.S. Department of Health and Human Services

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Total Diet Study - Analytical Extraction Steps, Pesticides and Industrial Chemicals

CFSAN/Office of Plant and Dairy Foods and Beverages
October 2000

Code Extraction Method Description
003 PAM I 304 E1-E5 + C1, 6 + 15 + 50% EE/PE eluants
009 PAM I 303 E1-E5 + C1, 6 + 15 + 50% EE/PE eluants
012 PAM I 303 E1-E5 + C2, MeCl2 eluants 1 + 2 + 3
015 PAM I 302 E1, no cleanup (see 046 for dry products)
023 PAM I 402 E1-E7 + C1
034 PAM I 304 E1-E5 + C6
038 PAM I 302 E2-E3, no cleanup
040 PAM I 403 E1 + C1; use with Detn Code 24
042 PAM I 302 E2-E3 + C1
450 TDS SOP KCP-1 milk products, SOP E1, GPC, F1 (Florisil)
451 TDS SOP KCP-1 fatty products, SOP E2, GPC, F1 (Florisil)
452 TDS SOP KCP-1 meat products, SOP E3, GPC, F1 (Florisil)
453 TDS SOP KCP-2 nonfatty products, SOP E4, C1
454 TDS SOP KCP-2 nonfatty products, SOP E4, C1, F2 (Florisil)
455 TDS SOP KCP-2 nonfatty products, SOP E4, C1, F3 (Florisil)
456 TDS SOP KCP-2 nonfatty products, SOP E4, GPC, C3
457 TDS SOP KCP-2 nonfatty products, SOP E4, GPC, C3, F2 (Florisil)
458 TDS SOP KCP-2 nonfatty products, SOP E4, GPC, C3, F3 (Florisil)
459 TDS SOP KCP-2 nonfatty products, SOP E5, GPC, C2
460 TDS SOP KCP-2 nonfatty products, SOP E5, GPC, C2, F2 (Florisil)
461 TDS SOP KCP-1 oilseed, SOP E6, GPC, F1 (Florisil)
462 TDS SOP KCP-1 infant formula, SOP E7, GPC, F1 (Florisil)
463 TDS SOP KCP-1 butter/oil, SOP E8, GPC, F1 (Florisil)
464 TDS SOP KCP-1 other fatty products, SOP E9, GPC, F1 (Florisil)
465 TDS SOP KCP-2 water, SOP E10
466 TDS SOP KCP-2 nonfatty products, SOP C4
467 TDS SOP KCP-2 sugars, SOP C4, F3 (Florisil)
468 TDS SOP KCP-7 carbamate pesticides
469 TDS SOP KCP-10, method for volatile organic compounds
470 TDS SOP KCP-1 selected fatty acid products, SOP SFE, GPC, F1 (Florisil)
600 PAM I 404 E1
611 JAOAC (1989), 72, 975-979 method for ETU/TD SOP KCP-8